WebMar 25, 2012 · A spectrophotometric method is developed for the determination of dissolved tri-n butyl phosphate (TBP) in aqueous streams of Purex process used in nuclear fuel reprocessing. The method is based on the formation of phosphomolybdate with added ammonium molybdate followed by reduction with hydrazine sulphate in acid medium. … WebThe following example describes the determination of phosphorus. A sample containing the phosphate is mixed with an acid solution of Mo VI, for example ammonium molybdate, to produce PMo 12O3− 40, which has an α- Keggin structure. This anion is then reduced by, for example, ascorbic acid or SnCl 2, to form the blue coloured β-keggin ion, PMo 12O7−
A New, Sensitive Determination of Phosphate
WebApr 28, 2024 · Water quality-determination of total phosphorus- ammonium molybdate spectrophotometric method was used to measure the dissolved phosphorus in the supernatant, and soil-determination of total phosphorus by alkali fusion Mo-Sb Anti spectrophotometric method for the adsorption of phosphorus in the sediment. WebTo prepare molybdenum liquid for determining the phosphate ion, dissolve 50 g of ammonium sulphate in 450 ml of a 68% nitric acid solution and 150 g of ammonium molybdate in 400 ml of distilled water. Cool the second solution to room temperature and pour it into the first one with constant stirring. smh travel insurance
Vanadate-molybdate reagent p.a., for phosphate determination
WebA quantitative method to determine the amount of phosphate present in samples, such as boiler feedwater, is as follows. A measured amount of boiler water is poured into a mixing … WebA simple spectrophotometric method has been developed for the determination of phosphate dissolved in soil and water. The method is based on the formation of … WebWhen ammonium molybdate solution is added to a solution of phosphate containing conc. H 2 SO 4 it produces a yellow crystalline precipitation of ammonium phospho-molybdate. … risk of rain 2 best artifact